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Exploris_PSB

Exploris_PSB

QC Annotation

 
Mass calibration

positive mode: passed

-LBC		2024-06-262024-06-26Instrumentation ChangeExploris_PSB2024-06-262024-06-26
Mass calibration

positive mode: passed

-LBC		2024-06-242024-06-24Instrumentation ChangeExploris_PSB2024-06-242024-06-24
Mass calibration

positive mode: passed

-LBC		2024-06-182024-06-18Instrumentation ChangeExploris_PSB2024-06-182024-06-18
Full system calibration.

positive mode: passed
negative mode: passed

-LBC		2024-06-032024-06-03Instrumentation ChangeExploris_PSB2024-06-032024-06-03
Mass calibration

positive mode: passed
negative mode: passed

-LBC		2024-02-132024-02-13Instrumentation ChangeExploris_PSB2024-02-132024-02-13
Mass and system calibration

positive mode: passed

-LBC		2024-02-062024-02-06Instrumentation ChangeExploris_PSB2024-02-062024-02-06
Mass axis calibration.
positive mode: passed
negative mode: passed

-LBC		2023-10-162023-10-16Instrumentation ChangeExploris_PSB2023-10-162023-10-16
Mass axis calibration
pos mode: passed
neg mode: passed

-LBC		2023-10-122023-10-12Instrumentation ChangeExploris_PSB2023-10-122023-10-12
Mass calibration.
positive mode: passed
negative mode: passed

LBC		2023-08-092023-08-10Instrumentation ChangeExploris_PSB2023-08-092023-08-09
Cleaned ion funnel, lens stack, and exit lens of bent flatapole.

-LBC		2023-05-04 Instrumentation ChangeExploris_PSB2023-05-042023-05-04
Mass and system calibration
pos mode: passed
neg mode: passed

LBC		2023-03-24 Instrumentation ChangeExploris_PSB2023-03-242023-03-24
Trap column: PepMap 100 75um x 2cm C18
SN 20344516

Analytical column: PepMap RSLC C18 75um x 25cm
SN C20415505		2023-03-24 Instrumentation ChangeExploris_PSB2023-03-242023-03-24
Mass axis calibratriuon
positive mode: passed
negative mode: passed

LBC		2022-11-14 Instrumentation ChangeExploris_PSB2022-11-152022-11-15
Mass axis calibration
positive mode: passed
negative mode: passed

LBC		2022-10-31 Instrumentation ChangeExploris_PSB2022-10-312022-10-31
Mass spectrometer calibration
system calibration positive mode: pass
system calibration negative mode: pass

LBC		2022-10-28 Instrumentation ChangeExploris_PSB2022-10-282022-10-28
Installed analytical column
PepMap RSLC C18
2um 100A 75um x 25cm
Part No. ES902
SN C20298278

LBC		2022-07-28 Analytical or Trap Column ChangeExploris_PSB2022-07-282022-07-28
positive mode mass calibration passed.
negative mode mass calibration passed.

LBC		2022-07-28 Instrumentation ChangeExploris_PSB2022-07-282022-07-28
MA10084N was moved from Toxicology bldg to Plant Sciences, room 2354.

Diagnostics for current status were performed on 6/7/22. All tests and calibrations passed.

Instrument was installed and powered up by Leonard Collins on 7/22/22.

Instrument was calibrated in positive and negative mode and ion optics tests performed on 7/25/22. All calibrations and tests passed.

Relevant documents uploaded to Mendix.		2022-07-25 Instrumentation ChangeExploris_PSB2022-07-252022-07-25
Removed old trap column. Connected new Acclaim PepMap 100, 75 um x 2 cm C18, 3 um particle.

SN: 20346011

Prepared new mobile phases and IPA/water wash solvent.		2022-07-25 Analytical or Trap Column ChangeExploris_PSB2022-07-252022-07-25
Analytical column replaced.
SN: C20298260
LBC		2022-04-26 Analytical or Trap Column ChangeExploris_PSB2022-04-262022-04-26
Mass axis calibrated.
positive mode: success
negative mode: success
LBC		2022-04-26 Instrumentation ChangeExploris_PSB2022-04-262022-04-26
Trap column replaced:
75um x 2cm C18 3um Acclaim PepMap 100
SN 20211630
LBC		2021-10-22 Analytical or Trap Column ChangeExploris_PSB2021-10-222021-10-22
Full calibration: positive mode passed
Mass Cal only: negative mode passed
LBC		2021-10-22 Instrumentation ChangeExploris_PSB2021-10-222021-10-22
Change new MP A and MP B2021-09-29 Solvent modificationExploris_PSB2021-09-292021-09-29
Posiive mode mass cal and system cal

YCC		2021-09-29 Instrumentation ChangeExploris_PSB2021-09-292021-09-29
Mass axis calibration:
positive mode passed
negative mode passed
LBC		2021-08-24 Instrumentation ChangeExploris_PSB2021-08-242021-08-24
Both analytical and trap columns were changed in the morning of 7/14/21 by Hellena Bai.

Analytical column SN: C20151956
Trap column SN: 20211631

Easy Spray Temperature Control cable changed.

Last columns have been resting for a while		2021-07-14 Analytical or Trap Column ChangeExploris_PSB2021-07-142021-07-27
-Mass calibration in (+) and (-) mode, both are passed quickly
-solvent change		2021-07-14 Instrumentation ChangeExploris_PSB2021-07-142021-07-14
-Tune software update
-Quad clean
-Full calibration
----------
Jon Delgado
Field Service Engineer III
Unity Lab Services
Thermo Fisher Scientific
Customer Service: +1 (800) 532-4752
Jon.delgado@thermofisher.com | www.unitylabservices.com		2021-07-07 Instrumentation ChangeExploris_PSB2021-07-082021-07-08
Mass calibration (+ve and -ve).
Changed HCTT (high capacity transfer tube).
--TIW		2021-06-03 Instrumentation ChangeExploris_PSB2021-06-032021-06-03
Mass calibration: positive
Mass calibration: negative
LBC		2021-05-04 Instrumentation ChangeExploris_PSB2021-05-042021-05-04
Installed analytical column: SN B20132421
LBC
Last column quickly developed clogged tip.		2021-04-29 Analytical or Trap Column ChangeExploris_PSB2021-04-292021-04-29
Mass calibration: positive
Mass calibration: negative
LBC		2021-04-29 Instrumentation ChangeExploris_PSB2021-04-292021-04-29
Installed analytical column: SN B20088703
Installed trap column: SN 20078257
LBC		2021-04-19 Analytical or Trap Column ChangeExploris_PSB2021-04-192021-04-19
Full calibration: positive
Full calibration: negative
LBC		2021-04-19 Instrumentation ChangeExploris_PSB2021-04-202021-04-20
Mass calibration: positive
Mass calibration: negative
LBC		2021-03-31 Instrumentation ChangeExploris_PSB2021-03-312021-03-31
New trap and analytical columns installed:
Trap: Acclaim PepMap 100; SN 20211652
Analytical: PepMap RSLC C18; SN B20137165		2021-03-31 Analytical or Trap Column ChangeExploris_PSB2021-03-312021-03-31
Service by John Polese.
Action: Orbitrap block with CT assembly replaced
Reason: negative mode performance unstable		2021-03-17 Instrumentation ChangeExploris_PSB2021-03-262021-03-26
Used command "Refresh Solvents" on nanoLC. Added MPs to bottles.
LBC		2021-03-13 Instrumentation ChangeExploris_PSB2021-03-132021-03-13
Mass calibration: positive
Mass calibration: negative
LBC		2021-03-12 Instrumentation ChangeExploris_PSB2021-03-122021-03-12
Full calibration: positive
Full calibration: negative
LBC		2021-03-10 Instrumentation ChangeExploris_PSB2021-03-122021-03-12
Full calibration: positive
Mass calibration: negative
LBC		2021-02-19 Instrumentation ChangeExploris_PSB2021-02-192021-02-19
Mass axis calibrations:
positive mode: passed
negative mode: passed		2021-02-10 Instrumentation ChangeExploris_PSB2021-02-102021-02-10
Trouble with high pressure. Changed analytical column.
SN B20091064		2021-02-05 Analytical or Trap Column ChangeExploris_PSB2021-02-052021-02-05
Full calibration negative mode: passed.
Mass calibration positive mode: passed.
LBC		2021-02-05 Instrumentation ChangeExploris_PSB2021-02-052021-02-05
Changed trap column - possibly clogged due to Sombers' samples -
Trap SN 20211653
JRE		2021-02-04 Analytical or Trap Column ChangeExploris_PSB2021-02-042021-02-04
Re-attached trap and analytical columns:
Trap SN 20077939
Analytical B20088697		2021-01-22 Analytical or Trap Column ChangeExploris_PSB2021-01-222021-01-22
Calibrated mass axis:
positive mode successful
negative mode not successful (601 peak abundance too low)		2021-01-22 Instrumentation ChangeExploris_PSB2021-01-222021-01-22
Full PM performed by John Polese.
Finished 1/20/21.		2021-01-20 Instrumentation ChangeExploris_PSB2021-01-222021-01-22
Liu submitted 1 more sample. Re-attached analytical column.2020-12-23 Analytical or Trap Column ChangeExploris_PSB2020-12-232020-12-23
Calibrated mass axis, pos and neg mode.2020-12-23 Instrumentation ChangeExploris_PSB2020-12-232020-12-23
Removed analytical column for winter break storage. Nano flow set to 100 nL/min.2020-12-21 Analytical or Trap Column ChangeExploris_PSB2020-12-232020-12-23
Fully calibrated pos and neg2020-11-16 Instrumentation ChangeExploris_PSB2020-11-172020-11-17
Mass calibration pos and neg mode2020-11-07 Instrumentation ChangeExploris_PSB2020-11-072020-11-07
solvent refresh2020-10-28 Solvent modificationExploris_PSB2020-11-072020-11-07
Mass calibration pos and neg mode2020-10-28 Instrumentation ChangeExploris_PSB2020-11-072020-11-07
Tune software version upgraded to 2.0.182.18 by John Polese of Thermo.2020-10-28 Instrumentation ChangeExploris_PSB2020-11-092020-11-09
New trap and analytical column2020-10-13 Analytical or Trap Column ChangeExploris_PSB2020-10-132020-10-13
New Analytical column2020-10-06 Analytical or Trap Column ChangeExploris_PSB2020-10-062020-10-06
Full system and mass calibration (positive mode)2020-10-06 Instrumentation ChangeExploris_PSB2020-10-062020-10-06
Added solvent to MPA and MPB. Mobile phases freshly prepared on 9/11/20 by LBC.2020-09-18 Solvent modificationExploris_PSB2020-09-182020-09-18
Mass axis calibrations successful for positive and negative modes. LBC2020-09-18 Instrumentation ChangeExploris_PSB2020-09-182020-09-18
Changed analytical column (from Goshe project to a seasoned column, not brand new)2020-09-11 Analytical or Trap Column ChangeExploris_PSB2020-09-152020-09-15
Changed the trap column2020-09-03 Analytical or Trap Column ChangeExploris_PSB2020-09-032020-09-03
Change analytical column2020-08-24 Analytical or Trap Column ChangeExploris_PSB2020-08-252020-08-25
Changed trap column2020-08-22 Analytical or Trap Column ChangeExploris_PSB2020-08-222020-08-22
Solvents replaced2020-08-20 Solvent modificationExploris_PSB2020-08-212020-08-21
Mass calibration (Full positive)2020-08-20 Instrumentation ChangeExploris_PSB2020-08-212020-08-21
Mass calibration2020-07-19 Instrumentation ChangeExploris_PSB2020-07-232020-07-23
New column!!!2020-03-13 Analytical or Trap Column ChangeExploris_PSB2020-03-132020-03-13
Refreshed and degassed solvents2020-03-13 Solvent modificationExploris_PSB2020-03-132020-03-13
Easy nLC 1200 Full PM2020-03-12 Technician ChangeExploris_PSB2020-03-122020-03-12
Trap Column Changed2020-03-05 Analytical or Trap Column ChangeExploris_PSB2020-03-122020-03-12
Removed FAIMS2020-03-05 Instrumentation ChangeExploris_PSB2020-03-062020-03-12
Added FAIMS2020-02-28 Instrumentation ChangeExploris_PSB2020-03-062020-03-06
UPGRADE TO EXPLORIS 4802019-12-06 Instrumentation ChangeExploris_PSB2020-03-112020-03-11
Fresh solvents, full LC re-equilibration2019-10-10 Solvent modificationExploris_PSB2019-10-102019-10-10
New trap column2019-10-10 Analytical or Trap Column ChangeExploris_PSB2019-10-102019-10-10
Calibrated Instrument2019-08-31 Instrumentation ChangeExploris_PSB2019-09-012019-09-01
Brand new trap and brand new analytical column2019-08-10 Analytical or Trap Column ChangeExploris_PSB2019-08-102019-08-10
New solvents2019-08-10 Solvent modificationExploris_PSB2019-08-102019-08-10
Fresh trap column put on - in right orientation. Analytical column still old used one.2019-08-08 Analytical or Trap Column ChangeExploris_PSB2019-08-092019-08-09
Put on old analytical column and new trap column - trap column on backwards =(2019-08-06 Analytical or Trap Column ChangeExploris_PSB2019-08-092019-08-09

QC Annotation Type

 
Analytical or Trap Column ChangeIf anything with regard to the analytical column or trap column is changed or some metric is noted about one of these pieces
Exploris_PSB2019-08-092019-08-09
Instrumentation Change 
Shared2015-02-172019-08-08
Instrument Downtime 
Shared2023-06-122023-06-12
Reagent Change 
Shared2015-02-172018-10-25
Solvent modificationAny change in solvents.
Exploris_PSB2019-08-092019-08-09
Technician Change 
Shared2015-02-172018-10-25

ReplicateAnnotation

 
No data to show.